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Automated reagent preparation
We are convinced that you will find our products and services about our solutions for your work in Automated reagent preparation useful to ensure the quality of your daily analytical work in the lab. Here: Automated weighing
More Information Characterizing the effects of different reaction variables on hydrogenation performance can be challenging. Grab sampling is often a poor choice due to oxygen sensitivity, transient intermediates reactivity, and handling of high-pressure reactors. On the other hand, hydrogen uptake monitoring only provides information on the overall rate of hydrogenation; it does not provide component-specific information, which is required for good process understanding. Our solutions in Automated reagent preparation will boost efficiency and accuracy in your company. The development of probe-based ATR-FTIR spectroscopy has significantly improved the convenience of monitoring reactions under actual conditions. Measuring the key reaction components in situ and in real time further enhances understanding of reaction kinetics, rates, and mechanisms. If you want to learn more about Automated reagent preparation - analytics, just let us know. Our solutions will move your business. Automated reagent preparation. We are convinced that you will find our products and services about our solutions for your work in Automated reagent preparation useful to ensure the quality of your daily analytical work in the lab. Chemical process development is undergoing significant changes. Scientists in Autochem are feeling ever-increasing economic pressure to bring compounds to market faster. The use of automation, parallel tools, and a range of Automated reagent preparation - analytics - both off-line and in-situ - is changing the way research is done. In-situ technologies such as ReactIR™ provide the process development scientist an additional tool to optimize Automated weighing. Automated weighing. We proudly present our know-how regarding Automated weighing. ReactIR™ is used to directly measure the liquid phase during hydrogenations. The solid catalyst is often not observed in the spectra even though the dispersions can be completely opaque (due to carbon-black-supported metal catalysts) and gas bubbles do not interfere with the measurements. MultiMaxIR™ has greatly facilitated the fast and efficient optimization of hydrogenation parameters with a unique combination of in-situ ATR-FTIR monitoring and parallel automated high-pressure reactors. During scale up and manufacturing, MonARC™ increases batch-to batch-consistency by safely detecting real-time process variance and reaction endpoint. We are convinced that you will find our information on Automated reagent preparation useful to ensure the quality of your daily analytical work in the lab. Autochem. Robust Hastelloy® probe bodies and diamond and sapphire windows allow virtually any class of Automated reagent preparation to be measured. ReactIR options include ultra-long fibers, eliminating the need for dedicated facilities (e.g., purge and liquid nitrogen). This instrument to measure the Automated weighing can be in a control room far away from the sampling point, which is ideal for the pilot plant environment. As in FTIR, the peak height will be proportional to concentration, so kinetic profiles can be determined by monitoring component peaks over the course of the reaction. ConcIRT™ algorithms can also be easily applied to ReactIR reaction data to automatically provide spectra of the components and their kinetic behavior. If you want to learn more about Autochem - analytics, let us know. The Know-how of our capable serviceteam will help you. Over 25% of Automated reagent preparation steps during multiple-stage syntheses in the pharmaceutical and fine chemical industries involve hydrogenations. The specialty Automated weighing industry is also reliant on these processes. Heterogeneous catalytic hydrogenations are ideal in that the reaction can be tuned for best activity and selectivity, and afterwards the catalyst can be removed by simple filtration. The optimization of a hydrogenation process requires selection of multiple parameters such as the correct catalyst, temperature, pressure, solvent, additives, and substrate-to-catalyst ratio. |
